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Handheld SERS coupled with QuEChERs for the sensitive analysis of multiple pesticides in basmati rice

Food Science and Technology

Handheld SERS coupled with QuEChERs for the sensitive analysis of multiple pesticides in basmati rice

N. Logan, S. A. Haughey, et al.

Discover how a team from Queen's University Belfast harnessed the power of handheld surface-enhanced Raman spectroscopy to detect pesticide residues in Basmati rice. Their innovative method improves detection limits and promotes rapid, on-site testing, ensuring food safety in a dynamic agricultural landscape.

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Playback language: English
Abstract
This study reports the handheld detection of four pesticide residues (acephate, carbendazim, thiamethoxam, and tricyclazole) in Basmati rice using surface-enhanced Raman spectroscopy (SERS). Different SERS substrates were synthesized and evaluated. Detection limits in solvent ranged from 5 ppb to 75 ppb. QuEChERs acetate extraction was used to recover pesticide residues from rice. This method improved detection limits within the matrix, enabling detection of three out of four pesticides below the Maximum Residue Limits (MRLs) of 10 ppb. The multiplexing performance of handheld-SERS was also assessed. The study demonstrates the potential of handheld-SERS for rapid, on-site pesticide residue detection.
Publisher
npj | Science of Food
Published On
Jan 13, 2022
Authors
Natasha Logan, Simon A. Haughey, Lin Liu, D. Thorburn Burns, Brian Quinn, Cuong Cao, Christopher T. Elliott
Tags
pesticide residues
Basmati rice
surface-enhanced Raman spectroscopy
handheld device
food safety
QuEChERS extraction
detection limits
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